Polyethylene
(PE) is the primary material used for gas pipe applications. Because of its
flexibility, ease of joining and long-term durability, along with lower
installed cost and lack of corrosion, gas companies want to install PE pipe
instead of steel pipe in larger diameters and higher pressures. As a result,
rapid crack propagation (RCP) is becoming a more important property of PE
materials.
This
article reviews the two key ISO test methods that are used to determine RCP
performance (full-scale test and small-scale steady state test), and compare
the values obtained with various PE materials on a generic basis. It also
reviews the status of RCP requirements in industry standards; such as ISO 4437,
ASTM D 2513 and CSA B137.4. In addition, it reviews progress within CSA Z662
Clause 12 and the AGA Plastic Materials Committee to develop industry
guidelines based on the values obtained in the RCP tests to design against an
RCP incident.
Background
Although
the phenomenon of RCP has been known and researched for several years 1, the
number of RCP incidents has been very low. A few have occurred in the gas
industry in North America, such as a 12-inch SDR 13.5 in the U.S. and a 6-inch
SDR 11 in Canada, and a few more in Europe.
With
gas engineers desiring to use PE pipe at higher operating pressures (up to 12
bar or 180 psig) and larger diameters (up to 30 inches), a key component of a
PE piping material - resistance to rapid crack propagation (RCP) - becomes more
important.
Most of
the original research work conducted on RCP was for metal pipe. As plastic pipe
became more prominent, researchers applied similar methodologies used for metal
pipe on the newer plastic pipe materials, and particularly polyethylene (PE)
pipe 2. Most of this research was done in Europe and through the ISO community.
Rapid
crack propagation, as its name implies, is a very fast fracture. Crack speeds
up to 600 ft/sec have been measured. These fast cracks can also travel long
distances, even hundreds of feet. The DuPont Company had two RCP incidents with
its high-density PE pipe, one that traveled about 300 feet and the other that
traveled about 800 feet.
RCP
cracks usually initiate at internal defects during an impact or impulse event.
They generally occur in pressurized systems with enough stored energy to drive
the crack faster than the energy is released. Based on several years of RCP
research, whether an RCP failure occurs in PE pipe depends on several factors:
1.
Pipe size.
2.
Internal pressure.
3.
Temperature.
4.
PE material
properties/resistance to RCP.
5.
Pipe processing.
Typical
features of an RCP crack are a sinusoidal (wavy) crack path along the pipe, and
“hackle” marks along the pipe crack surface that indicate the direction of the
crack. At times, the crack will bifurcate (split) into two directions as it
travels along the pipe.
Test Methods
The RCP
test method that is considered to be the most reliable is the full-scale (FS)
test method, as described in ISO 13478. This method requires at least 50 feet
of plastic pipe for each test and another 50 feet of steel pipe for the
reservoir. It is very expensive and time consuming. The cost to obtain the
desired RCP information can be in the hundreds of thousands of dollars.
Due to
the high cost for the FS RCP test, Dr. Pat Levers of Imperial College developed
the small-scale steady state (S4) test method to correlate with the full-scale
test3. This accelerated RCP test uses much smaller pipe samples (a few feet)
and a series of baffles, and is described in ISO 13477. The cost of conducting
this S4 testing is still expensive, but less than FS testing. Several
laboratories now have S4 equipment. A photograph with this article shows the S4
apparatus used by Jana Laboratories.
Whether
conducting FS or S4 RCP testing, there are two key results used by the piping
industry; one is the critical pressure and the other is the critical
temperature.
The
critical pressure is obtained by conducting a series of FS or S4 tests at a
constant temperature (generally 0°C) and varying the internal pressure. At low pressures, where
there is insufficient energy to drive the crack, the crack initiates and
immediately arrests (stops). At higher pressures, the crack propagates (goes)
to the end of the pipe. The critical pressure is shown by the red line in
Figure 1 as the transition between arrest at low pressures and propagation at
high pressures. In this case, the critical pressure is 10 bar (145 psig).
Due to
the baffles in the S4 test, the critical pressure obtained must be corrected to
correlate with the FS critical pressure. There has been considerable research
within the ISO community conducted in this area. Dr. Philippe Vanspeybroeck of
Becetel chaired a working group - ISO/TC 138/SC 5/WG RCP - that conducted S4
and FS testing on several PE pipes 4. Based on their extensive research effort,
the WG arrived at the following correlation formula 5 to convert the S4
critical pressure (Pc,S4) to the FS critical pressure (Pc,FS):
Pc,FS =
3.6 Pc,S4 + 2.6 bar (1)
It is
important to note that this S4/FS correlation formula may not be applicable to
other piping materials, such as PVC or polyamide (PA). For example, Arkema has
conducted S4 and FS testing on PA-11 pipe and found a different correlation
formula for PA-11 pipe 6.
The
critical temperature is obtained by conducting a series of FS or S4 tests at a
constant pressure (generally 5 bar or 75 psig) and varying the temperature 7.
At high temperatures the crack initiates and immediately arrests. At low
temperatures, the crack propagates to the end of the pipe. The critical
temperature is shown by the red line in Figure 2 as the transition between
arrest at high temperatures and propagation at low temperatures. In this case,
the critical temperature is 35°F (2°C).
RCP In ISO
The
International Standards Organization (ISO) product standard for PE gas pipe,
ISO 4437, has included an RCP requirement for many years 8. This is because
there were some RCP failures in early generation European PE gas pipes, and the
Europeans had conducted considerable research on RCP in PE pipes. Also,
European gas companies were using large-diameter pipes and higher operating
pressures for PE pipes, both of which make the pipe more susceptible to RCP
failures.
Below
is the current requirement for RCP taken from ISO 4437:
Pc >
1.5 x MOP (2)
Where:
Pc = full scale critical pressure, psig
MOP =
maximum operating pressure, psig
Most
manufacturers use the S4 test to meet this ISO 4437 RCP requirement. If the
requirement is not met, then the manufacturer may use the FS test. Therefore,
the ISO 4437 product standard requires that RCP testing be done, and also
provides values for the RCP requirement.
RCP In
ASTM
Until
recently, ASTM D 2513 did not address RCP at all 9. The AGA Plastic Materials
Committee (PMC) requested that an RCP requirement be added to ASTM D 2513,
similar to the RCP requirement in the ISO PE gas pipe standard ISO 4437. The
manufacturers agreed to include a requirement in ASTM D 2513 that RCP testing
(FS or S4) must be performed. The ASTM product standard D 2513 does not include
any required values.
PMC has
agreed with this approach and will develop its own industry requirement in the
form of a “white paper.” 10 The first draft was just issued within PMC with the
following proposed requirement:
PC,FS
> leak test pressure.
Leak
test pressure = 1.5 X MOP.
RCP In CSA
CSA
followed the direction of ASTM. The product standard CSA B137.4 11 requires
that the RCP testing must be done. The values of the RCP test will be
stipulated in CSA Z662 Clause 12, which is the Code of Practice for gas
distribution in Canada. Clause 12 recently approved the requirement as shown
nearby.
12.4.3.6
Rapid Crack Propagation (RCP) Requirements
When
tested in accordance with B137.4 requirements for PE pipe and compounds, the
standard PE pipe RCP Full-Scale critical pressure shall be at least 1.5 times
the maximum operating pressure. If the RCP Small-Scale Steady State method is
used, the RCP Full-Scale critical pressure shall be determined using the
correlation formula in B137.4.
RCP Test Data
The
critical pressure is the pressure - below which - RCP will not occur. The
higher the critical pressure, the less likely the gas company will have an RCP
event. In most cases, as the pipe diameter or wall thickness increases, the
critical pressure decreases. Therefore, RCP is more of a concern with
large-diameter or thick-walled pipe. Following are some typical critical
pressure values for various generic PE materials. For most cases, the pipe size
tested is 12-inch SDR 11 pipe.
PE
Material S4 Critical Pressure (PC,S4) at 32°F (0°C)/Full Scale Critical
Pressure (PC,FS) @ 0°C
Unimodal
MDPE 1 bar (15 psig)/6.2 bar (90 psig)
Bimodal
MDPE 10 bar (145 psig) /38.6 bar (560 psig)
Unimodal
HDPE 2 bar (30 psig)/9.8 bar (140 psig)
Bimodal
HDPE (PE 100+) 12 bar (180 psig)/45.8 bar (665 psig)
In
general, the RCP resistance is greater for HDPE (high-density PE) than MDPE
(medium-density PE). However, there is a significant difference when comparing
a unimodal PE to a bimodal PE material, about a ten-fold difference.
Bimodal
PE technology was developed in Asia and Europe in the 1980s. This technology is
known to provide superior performance for both slow crack growth and RCP, as
evidenced by the table. For the bimodal PE 100+ materials used in Europe and
Asia, the S4 critical pressure minimum requirement is 10 bar (145 psig), which
converts to 560 psig operating pressure. This means that with these bimodal PE
100+ materials, RCP will not be a concern. Today, there are several HDPE resin
manufacturers that use this bimodal technology. Recently, a new bimodal MDPE
material was introduced for the gas industry 12,13 with a significantly higher
S4 critical pressure compared to unimodal MDPE - 10 bar compared to 1 bar.
Another
measure of RCP resistance is the critical temperature. This is defined as the
temperature above which RCP will not occur. Therefore, a gas engineer wants to
use a PE material with a critical temperature as low as possible. Although
critical temperature is not used as a requirement in the product standards, it
is an important parameter, and perhaps should be given more consideration.
Following is a table with some typical critical temperature values for various
generic PE materials. For most cases, the pipe size tested is 12-inch SDR 11
pipe.
PE
Material/Critical Temperature (TC) at 5 bar (75 psig)
Unimodal
MDPE 15°C (60°F)
Bimodal
MDPE -2°C (28°F)
Unimodal
HDPE 9°C (48°F)
Bimodal
HDPE -17°C (1°F)
Again,
we see that RCP performance for HDPE is slightly better than MDPE, but there is
a significant difference between bimodal PE and unimodal PE. The bimodal MDPE
and HDPE materials have the lowest critical temperatures, which means the
greatest resistance to RCP.
Conclusion
As gas
companies use PE pipe in more demanding applications, such as larger pipe
diameters and higher operating pressures, the resistance of the PE pipe to
rapid crack propagation (RCP) becomes more important. In this article we have
discussed the phenomenon of RCP and the two primary test methods used to
determine RCP resistance - the S4 test and the Full Scale test. We reviewed the
correlation formula between the FS test and S4 test for critical pressure. We
have also discussed the two primary results of RCP testing - the critical
pressure and the critical temperature.
ISO
standards were the first to recognize the importance of RCP, especially in
larger diameter pipe sizes, and incorporated RCP requirements in product
standards, such as ISO 4437. The Canadian standards soon followed, and an RCP
test requirement has been added to CSA B137.4. The required values for RCP
testing are being added to the CSA Code of Practice in CSA Z662 Clause 12 for
gas piping. ASTM just added an RCP requirement to its gas pipe standard ASTM D
2513. The corresponding AGA PMC project to develop RCP recommendations for
required values from RCP testing is in progress.
In this
article, we also discussed some results of RCP testing. In general, the HDPE
materials have slightly greater RCP resistance than MDPE materials used in the
gas industry. A more significant difference is observed when comparing unimodal
PE materials to bimodal PE materials. Existing data indicate that bimodal HDPE
materials show a significant increase in critical pressure compared to unimodal
HDPE materials and also have considerably lower critical temperature values.
In
addition, this bimodal technology has now just been introduced for MDPE. This
bimodal MDPE material also has a significantly higher S4 critical pressure (10
bar vs. 1 bar) and a lower critical temperature than unimodal MDPE materials.
With several PE resin manufacturers being able to produce bimodal PE materials,
it is likely that in the near future, all PE materials used for the gas
industry will be bimodal materials because of their superior RCP resistance.
“Rapid
Crack Propagation Increasingly Important in Gas Applications: A Status Report”,
Dr. Gene Palermo, http://pipelineandgasjournal.com/rapid-crack-propagation-increasingly-important-gas-applications-status-report
George Gilbert Mattew
Student ID. 155 12 061
Course: KL4220 Subsea Pipeline
Prof. Ir. Ricky Lukman Tawekal, MSE, Ph. D./ Eko Charnius Ilman, ST, MT
Ocean Engineering Program, Institut Teknologi Bandung
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